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By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Maurizio FERRARI CNR-IFN, Italy Mrityunjay SINGH NASA Glenn Research Center, USA

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Read or Download 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART J including: Symposium PDF

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Extra info for 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART J including: Symposium

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3A). Situation is different for the aminated H-NCDb sample which possess a well defined N1s peak deriving from the contribution of two distinct chemical bonds as reported in figure 3B. 7 eV. Based on this result, we suggest that the oxygen plays an important role in the amination of the diamond surface. 5 405 404 403 402 401 400 399 398 397 Binding Energy (eV) Fig. 3. XPS spectra of the N1s core line after the amination treatments of the (A) H-NCDa sample and of the (B) H-NCDb sample. Although the chemical processes behind the grafting of amino-groups in presence of oxygen remain still unclear, we can assert that oxygen takes part to the functionalization increasing the grafting efficiency.

The high specific surface area (300 m2/g) was observed in the samples synthesized by this route [5]. Figure 3 SEM of pseudoboehmite after drying at 70o C/24h. Pietro VINCENZINI, Maurizio FERRARI and Mrityunjay SINGH 31 Measurements of the composite properties Using naked eyes it could be observed that the composite N99P01-20 is the more homogeneous composite. The results of the impact energy absorbed by the specimen during failure show that the addition of pseudoboehmite increased the izod test results (Figure 4).

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